de
en
Schliessen
Detailsuche
Bibliotheken
Projekt
Impressum
Datenschutz
zum Inhalt
Detailsuche
Schnellsuche:
OK
Ergebnisliste
Titel
Titel
Inhalt
Inhalt
Seite
Seite
Im Dokument suchen
Paneff, Florian: Elastic properties of Carbon nanomembranes and graphene: theory and experiment. 2021
Inhalt
Introduction
Carbon Nanomembranes (CNMs)
Self Assembled Monolayers (SAMs)
Electron Induced Cross Linking and CNMs
Theory of Bulge Test and Nanoindentation
Elastic Testing of 2D Materials
Stress and Strain
Bulge Test and Nanoindentation
Bulge Test Theory
Overview of Common Descriptions of a Pressurized Membrane
Small and Large Deflection Limit of a Uniformly Pressurized Membrane
Beams's Model to Describe the Bulge Test
Hencky's Solution for the Large Deflection Limit
Behavior of a Membrane with Initial Tension in the Intermediate Regime
Impact of the Assumption of a Uniformly Lateral Load
The Influence of Finite Strains
The Influence of Bending Stiffness
Conclusions
Nanoindentation Theory
Large Deflection Limit
Small Deflection Limit
Intermediate Range
Conclusions
2D modulus
Methods
Atomic Force Microscopy (AFM)
Force Curve
AFM Bulge Test and Nanoindentation
Helium Ion Microscopy (HIM)
X-ray Photoelectron Spectroscopy (XPS)
Sader Method for the Determination of the Spring Constant of the Cantilever
Experimental
Sample Preparation
SAM Preparation
Electron Irradiation
Sample Transfer
Critical Point Drying
CVD Graphene
Execution of Bulge Test and Nanoindentation
Cantilever Choice
Substrate and Optimal Membrane Diameter
Experimental Setup
Determination of the Central Point of the Membrane
Execution of the Bulge Test Experiment
Execution of the Nanoindentation Experiment
Data Analysis
Results
Determination of the AFM Tip Radius
Calibration Measurements on CVD Graphene
Quantitative Analysis and Discussion
2D Modulus and Young's Modulus of Different CNMs
TPT
ODT
Pyrolized TPT
PVBP and Pyrolized PVBP
Initial Tension
Uncertainty Estimation
Bulge Test
Nanoindentation
Summary of all Materials
Conclusions of the Thesis
Bibliography
Declaration of academic honesty
Mathematica Source Code for the Bulge Test Theory